b5a67555-ae07-3623-e054-002128a47908
English
dataset
British Geological Survey
+44 115 936 3100
Environmental Science Centre,Keyworth
NOTTINGHAM
NOTTINGHAMSHIRE
NG12 5GG
United Kingdom
enquiries@bgs.ac.uk
pointOfContact
2023-05-24
UK GEMINI
2.3
http://data.bgs.ac.uk/id/dataHolding/13607694
Intra-crystalline protein degradation dating of proboscidean enamel from the UK (NERC Grant NE/K500987/1)
2020-11-27
creation
http://data.bgs.ac.uk/id/dataHolding/13607694
The concentration of both L and D amino acid isomers was determined by HPLC (High-performance liquid chromatography) for multiple amino acids. 30 samples of proboscidean enamel were taken from the collections at BGS. Samples of enamel (~30 mg) was removed from the teeth of proboscideans using a small electric drill. All of the samples were from UK sites dating to the Quaternary. These samples were used to build a regional geochronology based on the extent of racemisation of amino acids from the intra-crystalline fraction (Dickinson, 2018). Thesis http://etheses.whiterose.ac.uk/22261. A published paper 'A new method for enamel amino acid racemization dating: A closed system approach' is also available; https://doi.org/10.1016/j.quageo.2018.11.005
Marc Dickinson
University of York
Chemistry Department
York
YO10 5DD
not available
originator
Enquiries
British Geological Survey
0115 936 3143
0115 936 3276
Environmental Science Centre, Nicker Hill, Keyworth
NOTTINGHAM
NOTTINGHAMSHIRE
NG12 5GG
United Kingdom
enquiries@bgs.ac.uk
distributor
Enquiries
British Geological Survey
0115 936 3143
0115 936 3276
Environmental Science Centre, Nicker Hill, Keyworth
NOTTINGHAM
NOTTINGHAMSHIRE
NG12 5GG
United Kingdom
enquiries@bgs.ac.uk
pointOfContact
notApplicable
https://resources.bgs.ac.uk/images/geonetworkThumbs/b5a67555-ae07-3623-e054-002128a47908.png
Geology
GEMET - INSPIRE themes
2008-06-01
publication
Racemization dating
Age determination methods
Geochronology
BGS Thesaurus of Geosciences
2011
revision
NERC_DDC
otherRestrictions
licenceOGL
Available under the Open Government Licence subject to the following acknowledgement accompanying the reproduced NERC materials "Contains NERC materials ©NERC [year]"
otherRestrictions
The copyright of materials derived from the British Geological Survey's work is vested in the Natural Environment Research Council [NERC]. No part of this work may be reproduced or transmitted in any form or by any means, or stored in a retrieval system of any nature, without the prior permission of the copyright holder, via the BGS Intellectual Property Rights Manager. Use by customers of information provided by the BGS, is at the customer's own risk. In view of the disparate sources of information at BGS's disposal, including such material donated to BGS, that BGS accepts in good faith as being accurate, the Natural Environment Research Council (NERC) gives no warranty, expressed or implied, as to the quality or accuracy of the information supplied, or to the information's suitability for any use. NERC/BGS accepts no liability whatever in respect of loss, damage, injury or other occurence however caused.
Available under the Open Government Licence subject to the following acknowledgement accompanying the reproduced NERC materials "Contains NERC materials ©NERC [year]"
textTable
English
geoscientificInformation
ISO 3166_1 alpha-3
2009
revision
ENG
British Geological Survey Gazetteer: Geographical hierarchy from Geosaurus
1979
creation
ENGLAND [id=150000]
0.0700
1.7000
51.4400
52.9200
2017-05-08
2018-07-01
Images (JPEG)
MS Excel
Enquiries
British Geological Survey
0115 936 3143
0115 936 3276
Environmental Science Centre, Nicker Hill, Keyworth
NOTTINGHAM
NOTTINGHAMSHIRE
NG12 5GG
United Kingdom
enquiries@bgs.ac.uk
distributor
http://etheses.whiterose.ac.uk/22261
information
https://doi.org/10.1016/j.quageo.2018.11.005
information
https://webapps.bgs.ac.uk/services/ngdc/accessions/index.html#item139845
Data
download
dataset
dataset
INSPIRE Implementing rules laying down technical arrangements for the interoperability and harmonisation of Geology
2011
publication
See the referenced specification
false
Commission Regulation (EU) No 1089/2010 of 23 November 2010 implementing Directive 2007/2/EC of the European Parliament and of the Council as regards interoperability of spatial data sets and services
2010-12-08
publication
See http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2010:323:0011:0102:EN:PDF
false
Samples of enamel (~30 mg) were powdered and exposed to NaOCl (12%) for 72 h. The NaOCl was removed and the powdered enamel was washed 5X with water and 1X with MeOH. Powdered enamel samples were split into 2 fractions. One sample was treated for their free amino acid (FAA) content and the other their total hydrolysable amino acid (THAA) content. THAA samples were dissolved in HCl (7M) and heated at 110 ̊C for 24 h. THAA samples were re-dissolved in HCl (1 M, 20 μLmg−1) and FAA samples were demineralised in HCl (1 M, 25 μLmg−1). KOH (1 M, 28 μLmg−1) was added to the acidified solutions. The sample was centrifuged for 10 min causing a clear supernatant to form above a gel; the biphasic separation. The supernatant was extracted and dried by centrifugal evaporation and analysed by HPLC. All methods are outlined in Dickinson et al., 2019.