The datasets contains two sets of three dimensional images of Ketton carbonate core of size 5 mm in diameter and 11 mm in length scanned at 7.97µm voxel resolution using Versa XRM-500 X-ray Microscope. The first set includes 3D dataset of dry (reference) Ketton carbonate. The second set includes 3D dataset of reacted Ketton carbonate using hydrochloric acid.